4-(溴甲基)苯甲酸乙酯合成路线 （共 44 条）
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane 2.5 h; Reflux;
参考文献
Ding, Derong; Yan, Guang
Chinese Journal of Chemistry, 2012 , vol. 30, # 8 p. 1906 - 1908
反应条件
sodium hydrogencarbonate T=20°C; Esterification; 4 h;
参考文献
Konya, Klara G.; Paul, Thomas; Lin, Shuqiong; Lusztyk, Janusz; Ingold
Journal of the American Chemical Society, 2000 , vol. 122, # 31 p. 7518 - 7527
反应条件
N-bromosuccinmide in tetrachloromethane
参考文献
British Biotech Pharmaceuticals Limited
Patent: US5428168 A1, 1995 ;
反应条件
N-bromosuccinmide in acetonitrile T=20°C; 0.416667 h; Flow reactorIrradiation;
参考文献
Cantillo, David; De Frutos, Oscar; Rincon, Juan A.; Mateos, Carlos; Oliver Kappe
Journal of Organic Chemistry, 2014 , vol. 79, # 1 p. 223 - 229
反应条件
1: 96 percent / Et3N / CH2Cl2 / 18 h 2: N-bromosuccinimide View Scheme
参考文献
Titley
Journal of the Chemical Society, 1928 , p. 2576
反应条件
1: 93 percent / SOCl2 / 3 h / Heating 2: 88 percent / NaHCO3 / 4 h / 20 °C View Scheme
参考文献
Konya, Klara G.; Paul, Thomas; Lin, Shuqiong; Lusztyk, Janusz; Ingold
Journal of the American Chemical Society, 2000 , vol. 122, # 31 p. 7518 - 7527
参考文献
G. D. Searle and Co.
Patent: US4804658 A1, 1989 ;
参考文献
G. D. Searle and Co.
Patent: US4804658 A1, 1989 ;
参考文献
G. D. Searle and Co.
Patent: US4804658 A1, 1989 ;
反应条件
1: sulfuric acid / 8 h / |Reflux 2: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 2.5 h / |Reflux View Scheme
参考文献
Sun, Libo; Xing, Hongzhu; Liang, Zhiqiang; Yu, Jihong; Xu, Ruren
Chemical Communications, 2013 , vol. 49, # 95 p. 11155 - 11157
