N-[双(甲硫基)亚甲基]对甲苯磺酰胺合成路线 （共 6 条）
反应条件
sodium hydroxide 1.) DMF, r.t., 2 h, 2.) r.t., 2 h; Yield given. Multistep reaction;
参考文献
Shi, Zhi-Bing; Zhao, Dan; Huang, Yan-Yan; Du, Yun; Cao, Xiang-Rong; Gong, Zhu-Nan; Zhao, Rui; Li, Jian-Xin
Chemical and Pharmaceutical Bulletin, 2012 , vol. 60, # 12 p. 1574 - 1580
反应条件
1: KOH / dimethylformamide 2: AcNMe2 View Scheme
参考文献
Field,L.; Buckman,J.D.
Journal of Organic Chemistry, 1968 , vol. 33, # 10 p. 3865 - 3871
反应条件
N,N-dimethyl acetamide
参考文献
Field,L.; Buckman,J.D.
Journal of Organic Chemistry, 1968 , vol. 33, # 10 p. 3865 - 3871
反应条件
(i) aq. NaOH, DMF, (ii) MeHal; Multistep reaction;
参考文献
Gompper,R.; Haegele,W.
Chemische Berichte, 1966 , vol. 99, p. 2885 - 2899
反应条件
in methanol cyclocondensation; 1) r.t., 24 h, 2) reflux, 20 h;
参考文献
Modzelewska-Banachiewicz; Matosiuk
Pharmazie, 1999 , vol. 54, # 8 p. 588 - 589
反应条件
1: tetrahydrofuran; H2O / 4 h / 60 °C 2: 89 percent / Celite; AgNO3; NH3 / acetonitrile / 20 °C View Scheme
参考文献
Szekely, Zoltan; Zakhariev, Sotir; Guarnaccia, Corrado; Antcheva, Nikolinka; Pongor, Sandor
Tetrahedron Letters, 1999 , vol. 40, # 23 p. 4439 - 4442
