1,1,1-三乙基-3,3,3-三甲基二硅氧烷合成路线 （共 41 条）
反应条件
[Ph3S][tBu2CarbCO2B(C6F5)3] in dichloromethane
T=20°C; 0.416667 h; UV-irradiation;
参考文献
UTI LIMITED PARTNERSHIP; PIERS, Warren Edward; KHALIMON, Andrey Yur'evich; VON MARWITZ, Adam John
Patent: WO2013/142956 A1, 2013 ;
Location in patent: Page/Page column 37; 39 ;
反应条件
[Ph3S][tBu2CarbCO2B(C6F5)3] in dichloromethane
T=20°C; 48.25 h; UV-irradiation;
参考文献
UTI LIMITED PARTNERSHIP; PIERS, Warren Edward; KHALIMON, Andrey Yur'evich; VON MARWITZ, Adam John
Patent: WO2013/142956 A1, 2013 ;
Location in patent: Page/Page column 37; 39 ;
反应条件
18-crown-6 ether; cesium fluoride in toluene
T=20°C; 0.5 h;
参考文献
Abele, Ramona; Abele, Edgars; Fleisher, Mendel; Grinberga, Solveiga; Lukevics, Edmunds
Journal of Organometallic Chemistry, 2003 , vol. 686, # 1-2 p. 52 - 57
反应条件
18-crown-6 ether; water; cesium fluoride in toluene
T=70°C; 19 h;
参考文献
Abele, Ramona; Abele, Edgars; Fleisher, Mendel; Grinberga, Solveiga; Lukevics, Edmunds
Journal of Organometallic Chemistry, 2003 , vol. 686, # 1-2 p. 52 - 57
反应条件
trifluoroacetic acid; Wilkinson's catalyst in tetrahydrofuran
T=130°C; 1 h;
参考文献
Park, Jung-Woo; Chang, Hoon-Jo; Jun, Chul-Ho
Synlett, 2006 , # 5 p. 771 - 775
反应条件
trifluoroacetic acid; Wilkinson's catalyst in toluene
T=130°C; 1 h;
参考文献
Park, Jung-Woo; Chang, Hoon-Jo; Jun, Chul-Ho
Synlett, 2006 , # 5 p. 771 - 775
反应条件
tri-ruthenium(0)dodecacarbonyl in benzene
T=60°C; 48 h;
参考文献
Seki, Yoshio; Takeshita, Kenji; Kawamoto, Kazuaki; Murai, Shinji; Sonoda, Noboru
Journal of Organic Chemistry, 1986 , vol. 51, # 20 p. 3890 - 3895
反应条件
diethyl ether; ethylmagnesium bromide
Kochen des Reaktionsprodukts mit verd.wss.HCl;
参考文献
Sommer; Kerr; Whitmore
Journal of the American Chemical Society, 1948 , vol. 70, p. 434
反应条件
N-methyl-formamide; acetoxytrimethylsilane
T=50°C; 14 h;
参考文献
Zhdanov, A. A.; Astapov, B. A.; Dmitricheva, N. A.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1793 - 1794,1592 - 1593
反应条件
trimethylsilyl formate
T=20°C; 1 h;
参考文献
Zhdanov, A. A.; Astapov, B. A.; Dmitricheva, N. A.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1793 - 1794,1592 - 1593
