2-氯-N-甲基-N-(4-硝基苯基)乙酰胺合成路线 (共 4 条)
反应条件
in toluene T=100°C; 2 h;
参考文献
Hennessy, Edward J.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2003 , vol. 125, # 40 p. 12084 - 12085
参考文献
Svetkin,Yu.V.
J. Gen. Chem. USSR (Engl. Transl.), 1965 , vol. 35, # 5 p. 834 - 836,837 - 839
反应条件
1: in toluene T=40 - 55°C; 2.5 h; 2: With hydrogen; palladium on activated charcoal in isopropyl alcohol; toluene T=20°C; P=750.075 Torr;
参考文献
WO2012/68441 A2, ;
Page/Page column 13; 14 ;
反应条件
in toluene T=40 - 55°C; 2.5 h; Product distribution / selectivity;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH
Patent: WO2009/71523 A1, 2009 ;
Location in patent: Page/Page column 4; 23-24 ;