N-[苄氧羰基]-D-谷氨酸 1-甲基酯合成路线 （共 7 条）
反应条件
trifluoroacetic acid in dichloromethane T=20°C; 1 h; Title compound not separated from byproducts;
参考文献
Van Heerbeek, Rieko; Kamer, Paul C. J.; Van Leeuwen, Piet N.M.W.; Reek, Joost N.H.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 2 p. 211 - 223
参考文献
Shirude, Pravin S.; Kumar, Vaijayanti A.; Ganesh, Krishna N.
Tetrahedron, 2004 , vol. 60, # 42 p. 9485 - 9491
反应条件
1: 95 percent / DMAP; DCC / CH2Cl2 / 2 h 2: TFA / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Van Heerbeek, Rieko; Kamer, Paul C. J.; Van Leeuwen, Piet N.M.W.; Reek, Joost N.H.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 2 p. 211 - 223
反应条件
1: 94 percent / NaHCO3 2: 82 percent / TsOH / benzene / Heating 3: 93 percent / NaOMe View Scheme
参考文献
Shirude, Pravin S.; Kumar, Vaijayanti A.; Ganesh, Krishna N.
Tetrahedron, 2004 , vol. 60, # 42 p. 9485 - 9491
反应条件
1: 82 percent / TsOH / benzene / Heating 2: 93 percent / NaOMe View Scheme
参考文献
Shirude, Pravin S.; Kumar, Vaijayanti A.; Ganesh, Krishna N.
Tetrahedron, 2004 , vol. 60, # 42 p. 9485 - 9491
参考文献
Marlborough,D.I.; Rydon,H.N.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1972 , p. 1 - 4
反应条件
1: Et3N / tetrahydrofuran
2: diethyl ether
3: 52 percent / [Rh(OAc)2]2 / benzene / Heating
4: 93 percent / NaBH4 / methanol
View Scheme
参考文献
Shirude, Pravin S.; Kumar, Vaijayanti A.; Ganesh, Krishna N.
Tetrahedron, 2004 , vol. 60, # 42 p. 9485 - 9491
