[1-(羟基甲基)环己基]甲醇合成路线 (共 27 条)
反应条件
1: 68 percent / pyridine 2: 72 percent / LiBr / 2-ethoxy-ethanol 3: 75 percent / Zn, ethylenediaminetetraacetic acid tetrasodium salt / ethanol View Scheme
参考文献
Shortridge et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 948
反应条件
phosphorus tribromide T=150°C;
参考文献
Fajgar, Radek; Pola, Josef
Journal of Organic Chemistry, 1993 , vol. 58, # 27 p. 7709 - 7717
参考文献
Backer; Winter
Recueil des Travaux Chimiques des Pays-Bas, 1937 , vol. 56, p. 492,506
Full Text Show Details
Shortridge et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 948
反应条件
sulfuric acid T=150 - 155°C; 12 h; Further byproducts given;
参考文献
Tetrahedron, , vol. 48, # 23 p. 4929 - 4936
反应条件
sulfuric acid T=150 - 155°C; 48 h; other substrates, other time, other concentration of H2SO4; MechanismProduct distribution;
参考文献
Tetrahedron, , vol. 48, # 23 p. 4929 - 4936
反应条件
sulfuric acid T=150 - 155°C; 48 h; Further byproducts given;
参考文献
Molnar, Arpad; Bucsi, Imre; Bartok, Mihaly
Tetrahedron, 1992 , vol. 48, # 23 p. 4929 - 4936
反应条件
sulfuric acid T=150 - 155°C; 48 h; other substrates, other time, other concentration of H2SO4; MechanismProduct distribution;
参考文献
Molnar, Arpad; Bucsi, Imre; Bartok, Mihaly
Tetrahedron, 1992 , vol. 48, # 23 p. 4929 - 4936
反应条件
sulfuric acid T=150 - 155°C; 12 h; Further byproducts given;
参考文献
Tetrahedron, , vol. 48, # 23 p. 4929 - 4936
反应条件
sulfuric acid T=150 - 155°C; 48 h; Further byproducts given;
参考文献
Tetrahedron, , vol. 48, # 23 p. 4929 - 4936
反应条件
sulfuric acid T=150 - 155°C; 48 h; other substrates, other time, other concentration of H2SO4; MechanismProduct distribution;
参考文献
Tetrahedron, , vol. 48, # 23 p. 4929 - 4936