[1-(羟基甲基)环己基]甲醇合成路线 (共 27 条)
参考文献
BASF
Patent: DE922648 , 1952 ;
反应条件
Yield given. Multistep reaction;
参考文献
Picard, P.; Leclercq, D.; Bats, J.-P.; Moulines, J.
Synthesis, 1981 , # 7 p. 550 - 551
反应条件
sulfuric acid
T=150 - 155°C; 12 h; Further byproducts given;
参考文献
Molnar, Arpad; Bucsi, Imre; Bartok, Mihaly
Tetrahedron, 1992 , vol. 48, # 23 p. 4929 - 4936
反应条件
sulfuric acid
T=150 - 155°C; 48 h; Further byproducts given;
参考文献
Molnar, Arpad; Bucsi, Imre; Bartok, Mihaly
Tetrahedron, 1992 , vol. 48, # 23 p. 4929 - 4936
反应条件
sulfuric acid
T=150 - 155°C; 48 h; other substrates, other time, other concentration of H2SO4; MechanismProduct distribution;
参考文献
Molnar, Arpad; Bucsi, Imre; Bartok, Mihaly
Tetrahedron, 1992 , vol. 48, # 23 p. 4929 - 4936
反应条件
3: LiAlH4
View Scheme
参考文献
Houk,J.; Whitesides,G.M.
Journal of the American Chemical Society, 1987 , vol. 109, p. 6825
参考文献
Houk,J.; Whitesides,G.M.
Journal of the American Chemical Society, 1987 , vol. 109, p. 6825