2-乙氧基-1,3-二甲基-苯合成路线 （共 22 条）
反应条件
sodium hydride in tetrahydrofuran; N,N-dimethyl-formamide T=85°C; 36 h;
参考文献
Van Der Boom, Milko E.; Liou, Shyh-Yeon; Ben-David, Yehoshoa; Shimon, Linda J. W.; Milstein, David
Journal of the American Chemical Society, 1998 , vol. 120, # 26 p. 6531 - 6541
反应条件
2-(di-t-butylphosphino)-1,1'-binaphthyl; palladium diacetate; caesium carbonate in toluene T=23°C; 29 h;
参考文献
Torraca; Huang; Parrish; Buchwald
Journal of the American Chemical Society, 2001 , vol. 123, # 43 p. 10770 - 10771
反应条件
calcium sulfate; anhydrous cobalt diacetate T=60°C; 5 h; Inert atmosphere;
参考文献
Carter Technologies; Carter, Melvin Keith
Patent: US2013/204037 A1, 2013 ;
Location in patent: Paragraph 0030 ;
反应条件
potassium carbonate 1.) THF, DMSO, reflux, 12 h, 2.) 200-220 deg C, 1 torr; Yield given. Multistep reaction;
参考文献
Abd-El-Aziz, A.S.; Lee, C. C.; Piorko, A.; Sutherland, R. G.
Journal of Organometallic Chemistry, 1988 , vol. 348, p. 95 - 108
反应条件
n-butyllithium; potassium tert-butylate 1) heptane, reflux, 20 h, 2) THF, 18 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Bates, Robert B.; Siahaan, Teruna J.; Suvannachut, Kessara
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1328 - 1334
反应条件
n-butyllithium; potassium tert-butylate Product distributionMechanism;
参考文献
Bates, Robert B.; Siahaan, Teruna J.; Suvannachut, Kessara
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1328 - 1334
反应条件
n-butyllithium; potassium tert-butylate; water; methoxybenzene 1) heptane, reflux, 20 h, 2) THF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bates, Robert B.; Siahaan, Teruna J.; Suvannachut, Kessara
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1328 - 1334
反应条件
n-butyllithium; potassium tert-butylate; water 1) heptane, reflux, 20 h, 2) THF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bates, Robert B.; Siahaan, Teruna J.; Suvannachut, Kessara
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1328 - 1334
反应条件
n-butyllithium; potassium tert-butylate 1) heptane, room temperature, 20 h, 2) THF; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Bates, Robert B.; Siahaan, Teruna J.; Suvannachut, Kessara
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1328 - 1334
反应条件
n-butyllithium; potassium tert-butylate 1) heptane, room temperature, 20 h, 2) THF; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Bates, Robert B.; Siahaan, Teruna J.; Suvannachut, Kessara
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1328 - 1334
