(8ci,9ci)-1-甲基-3-硝基-1H-1,2,4-噻唑合成路线 （共 11 条）
反应条件
lithium hydroxide in ethanol T=20 - 25°C; 200 h;
参考文献
Sukhanov; Lukin
Chemistry of Heterocyclic Compounds, 2005 , vol. 41, # 7 p. 861 - 865
反应条件
in toluene 1 h; Heating;
参考文献
Middleton; Monney; Parrick
Synthesis, 1984 , vol. NO. 9, p. 740 - 743
反应条件
methyl iodide T=3 - 21°C; 1.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Pevzner, M. S.; Kurenkov, A. A.; Trubitsin, A. E.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 9 p. 1470 - 1475
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 9 p. 1398 - 1403
参考文献
Kruglik, A. P.; Leshchev, S. M.; Rakhman'ko, E. M.; Bubel', O. N.; Asratyan, G. V.
J. Appl. Chem. USSR (Engl. Transl.), 1991 , vol. 64, # 8.2 p. 1721 - 1724,1576 - 1579
反应条件
T=3 - 21°C; 1.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Pevzner, M. S.; Kurenkov, A. A.; Trubitsin, A. E.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 9 p. 1470 - 1475
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 9 p. 1398 - 1403
反应条件
T=3 - 21°C; 1.5 h; Further byproducts given;
参考文献
Pevzner, M. S.; Kurenkov, A. A.; Trubitsin, A. E.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 9 p. 1470 - 1475
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 9 p. 1398 - 1403
反应条件
T=3 - 21°C; 1.5 h; Further byproducts given;
参考文献
Pevzner, M. S.; Kurenkov, A. A.; Trubitsin, A. E.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 9 p. 1470 - 1475
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 9 p. 1398 - 1403
反应条件
sodium hydroxide in ethanol T=20 - 25°C; 72 h; Product distribution; Further Variations:ReagentsTemperaturesSolventstime;
参考文献
Sukhanov; Lukin
Chemistry of Heterocyclic Compounds, 2005 , vol. 41, # 7 p. 861 - 865
参考文献
Sukhanov; Sakovich; Sukhanova; Lukin
Chemistry of Heterocyclic Compounds, 2005 , vol. 41, # 8 p. 994 - 998
反应条件
hydrazine; palladium 10 on activated carbon in methanol 1.5 h; Heating / reflux;
参考文献
Buettelmann, Bernd; Ceccarelli, Simona Maria; Jaeschke, Georg; Kolczewski, Sabine; Porter, Richard Hugh Philip; Vieira, Eric
Patent: US2006/160857 A1, 2006 ;
Location in patent: Page/Page column 55 ;
US 20060160857 A1
