N-甲基-4,4′-甲撑二苯胺合成路线 （共 8 条）
反应条件
hydrogenchloride in methanol; water 72 h; Heating;
参考文献
Katritzky, Alan R.; Lan, Xiangfu; Lam, Jamshed N.
Synthesis, 1990 , p. 341 - 346
反应条件
1: 60 percent / acetic acid / 0.25 h / Heating 2: 66 percent / conc. HCl / methanol; H2O / 72 h / Heating View Scheme
参考文献
Katritzky, Alan R.; Lan, Xiangfu; Lam, Jamshed N.
Synthesis, 1990 , p. 341 - 346
反应条件
in tetrahydrofuran; diethyl ether 1.) room temperature, 12 h, 2.) 50 deg C, 12 h;
参考文献
Barluenga, Jose; Campos, Pedro J.; Roy, Miguel A.; Asensio, Gregorio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1420 - 1426
反应条件
in methanol; water T=95°C; 3 h; quantitative determination of different condensation products, other time and temperature; Product distribution;
参考文献
Falke, P.; Tenner, R.; Knopp, H.
Journal fuer Praktische Chemie (Leipzig), 1986 , vol. 328, # 1 p. 142 - 148
反应条件
hydrogen; 5 Ru/Al2O3 in tetrahydrofuran T=83 - 105°C;
参考文献
DEGUSSA AG
Patent: WO2004/7425 A2, 2004 ;
Location in patent: Page 9-12 ;
反应条件
hydrogen; 5 Ru/Al2O3 in tetrahydrofuran T=90 - 110°C;
参考文献
DEGUSSA AG
Patent: WO2004/7425 A2, 2004 ;
Location in patent: Page 9-12 ;
反应条件
hydrogen; 5 Ru/Al2O3 in tetrahydrofuran
T=83 - 105°C;
参考文献
DEGUSSA AG
Patent: WO2004/7425 A2, 2004 ;
Location in patent: Page 9-12 ;
反应条件
hydrogen; 5 Ru/Al2O3 in tetrahydrofuran
T=90 - 110°C;
参考文献
DEGUSSA AG
Patent: WO2004/7425 A2, 2004 ;
Location in patent: Page 9-12 ;
