反应条件
1.1: NaHCO3; NBS / acetone; H2O / 2 h / -15 °C
1.2: furan; pyridine / acetone; H2O / 20 °C
2.1: NaClO2; 2-methyl-2-butene / 2-methyl-propan-2-ol; H2O; various solvent(s) / 2 h / 20 °C
3.1: Cl3C6H2COCl; Et3N / tetrahydrofuran / 2 h / 20 °C
3.2: 55 mg / DMAP / toluene / 5 h / 40 °C
4.1: 92 percent / CF3CO2H / CH2Cl2 / 1.5 h / 20 °C
5.1: NaBH4 / methanol / 1 h / 0 °C
View Scheme
参考文献
Kobayashi; Kumar; Kurachi; Acharya; Yamazaki; Kitazume
Journal of Organic Chemistry, 2001 , vol. 66, # 6 p. 2011 - 2018
