[(1S)-1-(重氮乙酰基)-2-甲基丁基]氨基甲酸芴甲酯合成路线 (共 2 条)
反应条件
1: Fmoc-NH-Ile-OH With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine in tetrahydrofuran; N,N-dimethyl-formamide 0.166667 h; 2: diazomethane in tetrahydrofuran; N,N-dimethyl-formamide T=0°C; 0.333333 h;
参考文献
Patil, Basanagoud S.; Vasanthakumar, Ganga-Ramu; Suresh Babu
Synthetic Communications, 2003 , vol. 33, # 18 p. 3089 - 3096
反应条件
in dichloromethane 1 h; Ambient temperature;
参考文献
Leggio, Antonella; Liguori, Angelo; Procopio, Antonio; Sindona, Giovanni
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 13 p. 1969 - 1971