2-(氯磺酰基)苯甲酸甲酯合成路线 （共 23 条）
反应条件
CuCl2; sodium nitrite in hydrogenchloride; water; acetic acid
参考文献
Bayer Aktiengesellschaft
Patent: US4725303 A1, 1988 ;
反应条件
phosphorus pentachloride T=95°C; 2.5 h;
参考文献
Waser, Jerome; Gaspar, Boris; Nambu, Hisanori; Carreira, Erick M.
Journal of the American Chemical Society, 2006 , vol. 128, # 35 p. 11693 - 11712
反应条件
water; chlorine in dichloromethane T=5 - 10°C; 1 h;
参考文献
Kim; Ko
Synthesis, 1992 , # 12 p. 1203 - 1204
反应条件
1: 1 h / Heating 2: 2.51 g / PCl5 / 2.5 h / 95 °C View Scheme
参考文献
Waser, Jerome; Gaspar, Boris; Nambu, Hisanori; Carreira, Erick M.
Journal of the American Chemical Society, 2006 , vol. 128, # 35 p. 11693 - 11712
参考文献
Maumee Devel.Co.
Patent: US2667503 , 1951 ;
参考文献
Basler Chem.Fabr.
Patent: DE124407 ;
参考文献
Cobb
American Chemical Journal, 1906 , vol. 35, p. 502
反应条件
pyridine; Rink amide resin; trifluoroacetic acid 1.) CH2Cl2, room temp., 15 h, 2.) CH2Cl2, 15 min; Yield given. Multistep reaction;
参考文献
Patil, Vikas; Kale, Manoj; Raichurkar, Anandkumar; Bhaskar, Brahatheeswaran; Prahlad, Dwarakanath; Balganesh, Meenakshi; Nandan, Santosh; Shahul Hameed
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 9 p. 2222 - 2225
反应条件
1: 80 percent / 98percent hydrazine hydrate, triethylamine / ethanol / 2 h / 0 °C 2: 92 percent / methanol / Heating View Scheme
参考文献
Vega; Diaz
Pharmazie, 1992 , vol. 47, # 10 p. 765 - 767
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=25°C;
参考文献
Bonfand, Eric; Motherwell, William B.; Pennell, Andrew M.K.; Uddin, Muhammed K.; Ujjainwalla, Feroze
Heterocycles, 1997 , vol. 46, # 1 p. 523 - 534
