(E)-N,N-二甲基十八碳-9-烯酰胺合成路线 (共 5 条)
反应条件
N-ethyl-N,N-diisopropylamine; [bis(2-methoxyethyl)amino]-sulfur trifluoride in dichloromethane T=0°C; 0.5 h;
参考文献
Kangani, Cyrous O.; Kelley, David E.
Tetrahedron Letters, 2005 , vol. 46, # 51 p. 8917 - 8920
反应条件
in benzene 1 h; Ambient temperature;
参考文献
Nagase; Kuwahara; Tominaga; Sugawara
Agricultural and Biological Chemistry, 1983 , vol. 47, # 1 p. 53 - 58
参考文献
Chebyshev,A.V. et al.
Journal of Organic Chemistry USSR (English Translation), 1977 , vol. 13, # 6 p. 1081 - 1084
Zhurnal Organicheskoi Khimii, 1977 , vol. 13, # 6 p. 1175 - 1178
反应条件
lithium aluminium tetrahydride in diethyl ether 6 h; Heating;
参考文献
Nagase; Kuwahara; Tominaga; Sugawara
Agricultural and Biological Chemistry, 1983 , vol. 47, # 1 p. 53 - 58
反应条件
1: Li<AlH2(OCH2CH2OMe)2> / diethyl ether; toluene
2: TsOH / ethanol
View Scheme
参考文献
Chebyshev,A.V. et al.
Journal of Organic Chemistry USSR (English Translation), 1977 , vol. 13, # 6 p. 1081 - 1084
Zhurnal Organicheskoi Khimii, 1977 , vol. 13, # 6 p. 1175 - 1178