4,4'-二羟基二苯硫醚合成路线 （共 32 条）
反应条件
silica bromide in dichloromethane T=20°C; 0.0833333 h; Inert atmosphere;
参考文献
Mohanazadeh, Farajollah; Veisi, Hojat; Sedrpoushan, Alireza; Zolfigol, Mohammad Ali; Golmohammad, Fereshteh; Hemmati, Saba; Hashemi, Majid
Journal of Sulfur Chemistry, 2014 , vol. 35, # 1 p. 7 - 13
反应条件
N(Et)4ClO4 in acetonitrile 2 h; Ambient temperatureworking pot.: 2.2 V vs SCE;
参考文献
Elothmani, Driss; Do, Quang Tho; Simonet, Jacques; Guillanton, Georges Le
Bulletin de la Societe Chimique de France, 1994 , vol. 131, p. 779 - 788
反应条件
AlCl3, aluminium chloride; thionyl chloride in diethyl ether T=25°C;
参考文献
Sun, Xiaoping; Haas, David; McWilliams, Samantha; Smith, Benjamin; Leaptrot, Katrina
Journal of Chemical Research, 2013 , vol. 37, # 12 p. 736 - 744
反应条件
potassium phosphate; copper(l) iodide; potassium thioacyanate in PEG-400 T=150°C; 20 h; Inert atmosphere;
参考文献
Li, Xiaokang; Yuan, Tangjun; Chen, Junmin
Chinese Journal of Chemistry, 2012 , vol. 30, # 3 p. 651 - 655
反应条件
sulfuric acid; acetic acid; isopentyl nitrite Diazotization.Eintragen der erhaltenen Diazoniumsalz-Loesung in wss. H2SO4 bei Siedetemperatur;
参考文献
Moore; Johnson
Journal of the American Chemical Society, 1935 , vol. 57, p. 1287
反应条件
N(Et)4ClO4; trichloroacetic acid in dichloromethane 2 h; Ambient temperatureworking pot.: 2.2 V vs SCE;
参考文献
Elothmani, Driss; Do, Quang Tho; Simonet, Jacques; Guillanton, Georges Le
Bulletin de la Societe Chimique de France, 1994 , vol. 131, p. 779 - 788
反应条件
1: lead (II)-oxide; sulfur / 135 - 145 °C 2: glacial acetic acid; concentrated sulfuric acid; isopentyl nitrite / Diazotization.Eintragen der erhaltenen Diazoniumsalz-Loesung in wss. H2SO4 bei Siedetemperatur View Scheme
参考文献
Moore; Johnson
Journal of the American Chemical Society, 1935 , vol. 57, p. 1287
参考文献
Bayer Aktiengesellschaft
Patent: US4252750 A1, 1981 ;
反应条件
sulfur; copper(l) iodide; lithium hydroxide hydrate in N,N-dimethyl-formamide T=100°C; 168 h; Inert atmosphere;
参考文献
Chen, Hsing-Ying; Peng, Wei-Te; Lee, Ying-Hsien; Chang, Yu-Lun; Chen, Yen-Jen; Lai, Yi-Chun; Jheng, Nai-Yuan; Chen, Hsuan-Ying
Organometallics, 2013 , vol. 32, # 19 p. 5514 - 5522
反应条件
sodium hydroxide; Na2S2 T=90°C;
参考文献
Okssengendler; Gerassimenko
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 3214
J. Gen. Chem. USSR (Engl. Transl.), 1957 , vol. 27, p. 3251
