6-甲氧基喹啉-3-羧酸乙酯合成路线 （共 5 条）
反应条件
sodium tetrahydroborate; palladium dichloride in methanol T=20°C; 1 h;
参考文献
Hanna-Elias, Amir; Manallack, David T.; Berque-Bestel, Isabelle; Irving, Helen R.; Coupar, Ian M.; Iskander, Magdy N.
Australian Journal of Chemistry, 2009 , vol. 62, # 2 p. 150 - 156
反应条件
1: With 1,10-phenanthroline; potassium carbonate; copper(l) chloride in acetonitrile T=80°C; 12 h; Schlenk techniqueSealed tubeInert atmosphere; 2: With 1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=80°C; 3 h; Schlenk techniqueSealed tubeInert atmosphere;
参考文献
Niu, Qingsheng; Mao, Hui; Yuan, Guodong; Gao, Jilong; Liu, Haiquan; Tu, Yawei; Wang, Xiaoxia; Lv, Xin
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 6 p. 1185 - 1192
反应条件
1: phosphorus tribromide / dichloromethane / 1 h / 20 °C 2: sodium azide / dimethyl sulfoxide / 16.5 h / 0 - 20 °C 3: trifluorormethanesulfonic acid / toluene / 3 h / 20 °C 4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / ethyl acetate / 0.08 h View Scheme
参考文献
Tummatorn, Jumreang; Thongsornkleeb, Charnsak; Ruchirawat, Somsak; Gettongsong, Tanita
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 9 p. 1463 - 1467
反应条件
1: trifluorormethanesulfonic acid / toluene / 3 h / 20 °C 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / ethyl acetate / 0.08 h View Scheme
参考文献
Tummatorn, Jumreang; Thongsornkleeb, Charnsak; Ruchirawat, Somsak; Gettongsong, Tanita
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 9 p. 1463 - 1467
反应条件
1: sodium azide / dimethyl sulfoxide / 16.5 h / 0 - 20 °C 2: trifluorormethanesulfonic acid / toluene / 3 h / 20 °C 3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / ethyl acetate / 0.08 h View Scheme
参考文献
Tummatorn, Jumreang; Thongsornkleeb, Charnsak; Ruchirawat, Somsak; Gettongsong, Tanita
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 9 p. 1463 - 1467
