1: With diphenyl diselenide; potassium carbonate; hydrazine hydrate in dimethyl sulfoxide T=70°C; Elimination; 7 h; 2: With oxalic acid in water; acetone T=20°C; Hydrolysis; 1 h; Further stages. Title compound not separated from byproducts.;
参考文献
Vasil'ev, Andrei; Engman, Lars
Journal of Organic Chemistry, 2000 , vol. 65, # 7 p. 2151 - 2162