(S,s)-n-苄基-3,4-反式-(n-boc)-二氨基吡咯烷合成路线 （共 6 条）
反应条件
in dichloromethane Ambient temperature;
参考文献
Lohray, Braj B.; Baskaran; Srinivasa Rao, Bonthu; Mallesham; Bharath; Yadi Reddy; Venkateswarlu; Sadhukhan, Ashok K.; Kumar, M. Sitaram; Sarnaik, Hemant M.
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 5 p. 525 - 528
反应条件
1: 95 percent / HN3; DEAD; PPh3 2: LiAlH4 / tetrahydrofuran / 0.5 h / Heating 3: 1.5 g / NaOH / H2O; dioxane / 2 h / 20 °C View Scheme
参考文献
Brouwer, Arwin J.; van Der Linden, Heiko J.; Liskamp, Rob M. J.
Journal of Organic Chemistry, 2000 , vol. 65, # 6 p. 1750 - 1757
反应条件
1: 67 percent / NaBH4; BF3*Et2O 2: 95 percent / HN3; DEAD; PPh3 3: LiAlH4 / tetrahydrofuran / 0.5 h / Heating 4: 1.5 g / NaOH / H2O; dioxane / 2 h / 20 °C View Scheme
参考文献
Brouwer, Arwin J.; van Der Linden, Heiko J.; Liskamp, Rob M. J.
Journal of Organic Chemistry, 2000 , vol. 65, # 6 p. 1750 - 1757
反应条件
1: 75 percent / Heating 2: 67 percent / NaBH4; BF3*Et2O 3: 95 percent / HN3; DEAD; PPh3 4: LiAlH4 / tetrahydrofuran / 0.5 h / Heating 5: 1.5 g / NaOH / H2O; dioxane / 2 h / 20 °C View Scheme
参考文献
Brouwer, Arwin J.; van Der Linden, Heiko J.; Liskamp, Rob M. J.
Journal of Organic Chemistry, 2000 , vol. 65, # 6 p. 1750 - 1757
反应条件
1: LiAlH4 / tetrahydrofuran / 0.5 h / Heating 2: 1.5 g / NaOH / H2O; dioxane / 2 h / 20 °C View Scheme
参考文献
Brouwer, Arwin J.; van Der Linden, Heiko J.; Liskamp, Rob M. J.
Journal of Organic Chemistry, 2000 , vol. 65, # 6 p. 1750 - 1757
反应条件
hydrogen; palladium dihydroxide in water; tert-butyl alcohol T=20°C; Hydrogenolysis; P=2250.23 Torr;
参考文献
Brouwer, Arwin J.; van Der Linden, Heiko J.; Liskamp, Rob M. J.
Journal of Organic Chemistry, 2000 , vol. 65, # 6 p. 1750 - 1757
