三甲基1,3,5-苯三羟酸酯合成路线 （共 67 条）
反应条件
in methanol T=120°C; Michael addition; 0.5 h; Microwave irradiation;
参考文献
Adams, Jeff; Hardin, Alison; Vounatsos, Filisaty
Journal of Organic Chemistry, 2006 , vol. 71, # 26 p. 9895 - 9898
参考文献
Snyder et al.
Journal of the American Chemical Society, 1939 , vol. 61, p. 3558
反应条件
in dichloromethane T=140°C; 120 h; Yield given. Title compound not separated from byproducts;
参考文献
Sepulveda-Arques, Jose; Alvarez de Laviada, M. Jose; Medio-Simon, Mercedes
Monatshefte fuer Chemie, 1990 , vol. 121, # 1 p. 81 - 84
反应条件
(CO)3Ni(PPh3)2 in benzene 2 h; Heating; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Schumann, Herbert; Rodewald, Gisbert
Journal of Chemical Research, Miniprint, 1982 , # 8 p. 2201 - 2228
反应条件
(CO)3Ni(PPh3)2 in benzene 2 h; Heating; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Schumann, Herbert; Rodewald, Gisbert
Journal of Chemical Research, Miniprint, 1982 , # 8 p. 2201 - 2228
反应条件
in n-heptane The soln. was refluxed for two hours under N2; separated by column chromy.. Recrystn. from hexane/diethyl ether at -80°C yielded brown crystals. Detected by IR, NMR, Elem. anal.;
参考文献
Muller, Fred; Koten, Gerard van; Vrieze, Kees; Heijdenrijk, Dick; Krijnen, Bert B.; Stam, Casper H.
Organometallics, 1989 , vol. 8, p. 41 - 48
反应条件
in toluene the mixt. in toluene was heated at 70°C for 24 h; solvent was removed, not sepd., detected by NMR spectra;
参考文献
Herberhold, Max; Yan, Hong; Milius, Wolfgang; Wrackmeyer, Bernd
Organometallics, 2000 , vol. 19, # 21 p. 4289 - 4294
反应条件
in chloroform the mixt. in CHCl3 was heated at reflux for 24 h; solvent was removed, not sepd., detected by NMR spectra;
参考文献
Herberhold, Max; Yan, Hong; Milius, Wolfgang; Wrackmeyer, Bernd
Organometallics, 2000 , vol. 19, # 21 p. 4289 - 4294
反应条件
in toluene the mixt. in toluene was heated at 70°C for 24 h; solvent was removed, not sepd., detected by NMR spectra;
参考文献
Herberhold, Max; Yan, Hong; Milius, Wolfgang; Wrackmeyer, Bernd
Organometallics, 2000 , vol. 19, # 21 p. 4289 - 4294
反应条件
in toluene the mixt. in toluene was heated at 70°C for 24 h; solvent was removed, not sepd., detected by NMR spectra;
参考文献
Herberhold, Max; Yan, Hong; Milius, Wolfgang; Wrackmeyer, Bernd
Organometallics, 2000 , vol. 19, # 21 p. 4289 - 4294
