4-(二苯基氨基)苯硼酸频那醇酯合成路线 （共 12 条）
反应条件
potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in dimethyl sulfoxide T=80°C; 6 h;
参考文献
Samsung Display Co., Ltd.
Patent: EP2535331 A1, 2012 ;
Location in patent: Page/Page column 29 ;
反应条件
potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in N,N-dimethyl-formamide T=80°C; 30 h; Inert atmosphere;
参考文献
Semiconductor Energy Laboratory Co., Ltd.
Patent: US2012/165523 A1, 2012 ;
Location in patent: Page/Page column 27 ;
反应条件
1: 4-(N,N-diphenylamino)-bromobenzene With n-butyllithium in tetrahydrofuran T=-78°C; 0.5 h; 2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran T=-78 - 20°C;
参考文献
Lee, Junghoon; Kim, Jonggi; Kim, Gyoungsik; Yang, Changduk
Tetrahedron, 2010 , vol. 66, # 48 p. 9440 - 9444
反应条件
1: 4-(N,N-diphenylamino)-bromobenzene With n-butyllithium in tetrahydrofuran T=-78 - -50°C; Cooling with acetone-dry ice; 2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran T=-78 - 20°C; 15 h; Cooling with acetone-dry ice;
参考文献
3M Innovative Properties Company
Patent: US7094902 B2, 2006 ;
Location in patent: Page/Page column 92-93 ;
反应条件
in acetone T=20°C; Inert atmosphere;
参考文献
Tsoi, Yuk-Tai; Zhou, Zhongyuan; Yu, Wing-Yiu
Organic Letters, 2011 , vol. 13, # 19 p. 5370 - 5373
反应条件
1.1: copper(l) iodide; 1,10-phenanthroline; potassium hydroxide / toluene / 48 h / Reflux 2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 - -40 °C 2.2: -78 - 20 °C View Scheme
参考文献
Pham, Van Chung; Huh, Geun; Kim, Jungahn; Choo, Dong Joon; Lee, Jae Yeol
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 5 p. 1781 - 1783
反应条件
1.1: copper(l) iodide; 1,10-phenanthroline; potassium hydroxide / toluene / 48 h / Reflux 2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 - -40 °C 2.2: -78 - 20 °C View Scheme
参考文献
Pham, Van Chung; Huh, Geun; Kim, Jungahn; Choo, Dong Joon; Lee, Jae Yeol
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 5 p. 1781 - 1783
反应条件
1.1: N-bromosuccinmide / N,N-dimethyl-formamide / 4 h / 0 °C 2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere 2.2: 13 h / -78 - 20 °C / Inert atmosphere View Scheme
参考文献
Shi, Liqi; He, Chao; Zhu, Defeng; He, Qingguo; Li, Yang; Chen, Yan; Sun, Yuxi; Fu, Yanyan; Wen, Dan; Cao, Huimin; Cheng, Jiangong
Journal of Materials Chemistry, 2012 , vol. 22, # 23 p. 11629 - 11635
反应条件
in toluene 10 h; Reflux;
参考文献
Ren, Shijie; Zeng, Danli; Zhong, Hongliang; Wang, Yaochuan; Qian, Shixiong; Fang, Qiang
Journal of Physical Chemistry B, 2010 , vol. 114, # 32 p. 10374 - 10383
参考文献
Song, Mi-Seon; Nguyen, Quynh Pham Bao; Song, Chang-Hyun; Lee, Duckhee; Chai, Kyu Yun
Molecules, 2013 , vol. 18, # 11 p. 14033 - 14041
