乙基3,7-二甲基-6-辛烯酸酯合成路线 （共 21 条）
反应条件
hydrogen; platinum in ethanol
参考文献
Odinokov, V. N.; Kukovinets, O. S.; Sakharova, N. I.; Tolstikov, G. A.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 1.1 p. 24 - 30
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 1 p. 31 - 38
反应条件
lithium iodide in N,N-dimethyl-formamide T=150°C; 4 h;
参考文献
Odinokov, V. N.; Kukovinets, O. S.; Sakharova, N. I.; Tolstikov, G. A.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 1.1 p. 24 - 30
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 1 p. 31 - 38
反应条件
hydrogen; palladium on activated charcoal
参考文献
Kanazawa, Yoshinori; Tsuchiya, Yasunori; Kobayashi, Kazuki; Shiomi, Takushi; Itoh, Jun-Ichi; Kikuchi, Makoto; Yamamoto, Yoshihiko; Nishiyama, Hisao
Chemistry - A European Journal, 2006 , vol. 12, # 1 p. 63 - 71
反应条件
manganese(IV) oxide; sodium acetate 5 h; Heating;
参考文献
Chikashita; Ishihara; Takigawa; Itoh
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 11 p. 3256 - 3261
反应条件
ethanol; sodium carbonate; Rhodium trichloride; triphenylphosphine 8.3 h; Heatingother catalysts;
参考文献
Grigg, Ronald; Mitchell, Thomas R. B.; Sutthivaiyakit, Somyote
Tetrahedron, 1981 , vol. 37, # 24 p. 4313 - 4319
反应条件
sodium ethanolate T=110°C;
参考文献
Bouveault; Blanc
Patent: DE164294 ;
Full Text Show Details
Bouveault; Gourmand
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1904 , vol. 138, p. 1701
Chem. Zentralbl., 1905 , vol. 76, # II p. 1701
反应条件
1: 84 percent / pyridine, piperidine / 3 h / 120 °C 2: 71 percent / sodium borohydride / methanol / 1.) 5 deg C, 15 min, 2.) 20 deg C, 0.5 h 3: 1.82 g / TsOH*Py / acetone; H2O / 2 h / Heating 4: 1.) butyllithium / 1.) THF, hexane, -78 deg C, 1 h, 2.)a) THF, hexane, -78 deg C, 1 h, b) 20 deg C, 15 h 5: 71 percent / lithium iodide / dimethylformamide / 4 h / 150 °C View Scheme
参考文献
Odinokov, V. N.; Kukovinets, O. S.; Sakharova, N. I.; Tolstikov, G. A.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 1.1 p. 24 - 30
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 1 p. 31 - 38
反应条件
1: 67 percent / KOH / ethane-1,2-diol; H2O; ethanol / 18 h / Heating 2: 86 percent / oxalyl chloride, pyridine / benzene / 2 h / Ambient temperature 3: 76 percent / triethyl amine / diethyl ether / 1 h / Ambient temperature 4: 82 percent / diethyl ether / Ambient temperature 5: 38 percent / acetonitrile / Irradiation View Scheme
参考文献
Charlton, James Leslie.; Lai, Hoi Kiong.; Lypka, Gerald Nicholas
Canadian Journal of Chemistry, 1980 , vol. 58, p. 458 - 462
反应条件
1: 42 percent / PBr3, pyridine / diethyl ether 2: 60 percent / dimethylsulfoxide 3: 67 percent / KOH / ethane-1,2-diol; H2O; ethanol / 18 h / Heating 4: 86 percent / oxalyl chloride, pyridine / benzene / 2 h / Ambient temperature 5: 76 percent / triethyl amine / diethyl ether / 1 h / Ambient temperature 6: 82 percent / diethyl ether / Ambient temperature 7: 38 percent / acetonitrile / Irradiation View Scheme
参考文献
Charlton, James Leslie.; Lai, Hoi Kiong.; Lypka, Gerald Nicholas
Canadian Journal of Chemistry, 1980 , vol. 58, p. 458 - 462
反应条件
1: 60 percent / dimethylsulfoxide 2: 67 percent / KOH / ethane-1,2-diol; H2O; ethanol / 18 h / Heating 3: 86 percent / oxalyl chloride, pyridine / benzene / 2 h / Ambient temperature 4: 76 percent / triethyl amine / diethyl ether / 1 h / Ambient temperature 5: 82 percent / diethyl ether / Ambient temperature 6: 38 percent / acetonitrile / Irradiation View Scheme
参考文献
Charlton, James Leslie.; Lai, Hoi Kiong.; Lypka, Gerald Nicholas
Canadian Journal of Chemistry, 1980 , vol. 58, p. 458 - 462
