乙基3,7-二甲基-6-辛烯酸酯合成路线 （共 21 条）
反应条件
1: LiAlH4 / diethyl ether 2: 42 percent / PBr3, pyridine / diethyl ether 3: 60 percent / dimethylsulfoxide 4: 67 percent / KOH / ethane-1,2-diol; H2O; ethanol / 18 h / Heating 5: 86 percent / oxalyl chloride, pyridine / benzene / 2 h / Ambient temperature 6: 76 percent / triethyl amine / diethyl ether / 1 h / Ambient temperature 7: 82 percent / diethyl ether / Ambient temperature 8: 38 percent / acetonitrile / Irradiation View Scheme
参考文献
Charlton, James Leslie.; Lai, Hoi Kiong.; Lypka, Gerald Nicholas
Canadian Journal of Chemistry, 1980 , vol. 58, p. 458 - 462
反应条件
1: 86 percent / oxalyl chloride, pyridine / benzene / 2 h / Ambient temperature 2: 76 percent / triethyl amine / diethyl ether / 1 h / Ambient temperature 3: 82 percent / diethyl ether / Ambient temperature 4: 38 percent / acetonitrile / Irradiation View Scheme
参考文献
Charlton, James Leslie.; Lai, Hoi Kiong.; Lypka, Gerald Nicholas
Canadian Journal of Chemistry, 1980 , vol. 58, p. 458 - 462
反应条件
1: 76 percent / triethyl amine / diethyl ether / 1 h / Ambient temperature 2: 82 percent / diethyl ether / Ambient temperature 3: 38 percent / acetonitrile / Irradiation View Scheme
参考文献
Charlton, James Leslie.; Lai, Hoi Kiong.; Lypka, Gerald Nicholas
Canadian Journal of Chemistry, 1980 , vol. 58, p. 458 - 462
反应条件
[C4C1im][MeCO2] T=20 - 70°C; 2.08333 h;
参考文献
Yu, Yinyin; Hua, Li; Zhu, Wenwen; Shi, Yu; Cao, Ting; Qiao, Yunxiang; Hou, Zhenshan
Synthetic Communications, 2013 , vol. 43, # 9 p. 1287 - 1298
反应条件
in acetonitrile Irradiation;
参考文献
Charlton, James Leslie.; Lai, Hoi Kiong.; Lypka, Gerald Nicholas
Canadian Journal of Chemistry, 1980 , vol. 58, p. 458 - 462
反应条件
chloro-trimethyl-silane; copper(l) chloride; lithium chloride; manganese (II) chloride 1.) THF, 0 deg C, 20 min, 2.) 0 to 20 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Cahiez, Gerard; Alami, Mouad
Tetrahedron Letters, 1990 , vol. 31, # 51 p. 7423 - 7424
反应条件
RhH(CO)(triphenylphosphine)3 72 h; Heating;
参考文献
Grigg, Ronald; Mitchell, Thomas R. B.; Sutthivaiyakit, Somyote
Tetrahedron, 1981 , vol. 37, # 24 p. 4313 - 4319
参考文献
Rochussen
Journal fuer Praktische Chemie (Leipzig), 1922 , vol. <2> 105, p. 122
反应条件
1: 82 percent / diethyl ether / Ambient temperature 2: 38 percent / acetonitrile / Irradiation View Scheme
参考文献
Charlton, James Leslie.; Lai, Hoi Kiong.; Lypka, Gerald Nicholas
Canadian Journal of Chemistry, 1980 , vol. 58, p. 458 - 462
反应条件
1: oxidation View Scheme
参考文献
Charlton, James Leslie.; Lai, Hoi Kiong.; Lypka, Gerald Nicholas
Canadian Journal of Chemistry, 1980 , vol. 58, p. 458 - 462
