1-(4-甲氧基-2-甲基-1,3-苯并噻唑-7-基)乙酮合成路线 （共 4 条）
反应条件
AlCl3, aluminium chloride in carbon disulfide 1.5 h; Reflux;
参考文献
InterMune, Inc.
Patent: US2011/152246 A1, 2011 ;
Location in patent: Page/Page column 139 ;
反应条件
1: triethylamine / 3 h / 0 - 20 °C 2: Lawesson's reagent / toluene / 3 h / 110 °C / Inert atmosphere 3: potassium hexacyanoferrate(III); sodium hydroxide / ethanol; water / 0.83 h / 90 °C 4: AlCl3, aluminium chloride / carbon disulfide / 1.5 h / Reflux View Scheme
参考文献
InterMune, Inc.
Patent: US2011/152246 A1, 2011 ;
反应条件
1: Lawesson's reagent / toluene / 3 h / 110 °C / Inert atmosphere 2: potassium hexacyanoferrate(III); sodium hydroxide / ethanol; water / 0.83 h / 90 °C 3: AlCl3, aluminium chloride / carbon disulfide / 1.5 h / Reflux View Scheme
参考文献
InterMune, Inc.
Patent: US2011/152246 A1, 2011 ;
反应条件
1: potassium hexacyanoferrate(III); sodium hydroxide / ethanol; water / 0.83 h / 90 °C 2: AlCl3, aluminium chloride / carbon disulfide / 1.5 h / Reflux View Scheme
参考文献
InterMune, Inc.
Patent: US2011/152246 A1, 2011 ;
