2-氯-N,N-二甲基乙酰胺合成路线 （共 38 条）
参考文献
Farbenfabr.Bayer
Patent: DE875807 , 1951 ;
参考文献
Nuretdinova, O. N.; Guseva, F. F.; Troitskaya, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 12 p. 2493 - 2495
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , vol. 40, # 12 p. 2858 - 2860
反应条件
triethylamine; sodium iodide in N,N-dimethyl-formamide Ambient temperature;
参考文献
Nielsen; Bundgaard
Journal of pharmaceutical sciences, 1988 , vol. 77, # 4 p. 285 - 298
参考文献
Hoegberg; Cassaday
Journal of the American Chemical Society, 1951 , vol. 73, p. 557
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Mandel'baum et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 283; engl. Ausg. S. 287
参考文献
Hoegberg; Cassaday
Journal of the American Chemical Society, 1951 , vol. 73, p. 557
Full Text View citing articles Show Details
Mandel'baum et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 283; engl. Ausg. S. 287
反应条件
sodium hydroxide; water; trichlorophosphate
参考文献
Upjohn Co.
Patent: GB869775 , 1959 ;
反应条件
potassium carbonate in acetonitrile
参考文献
Nitta, Aiko; Iura, Yosuke; Inoue, Hideki; Imaoka, Takayuki; Takahashi, Toshiya; Sato, Ippei; Morihira, Koichiro; Kubota, Hirokazu; Morokata, Tatsuaki; Takeuchi, Makoto; Ohta, Mitsuaki; Tsukamoto, Shin-Ichi
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 22 p. 6876 - 6881,6
反应条件
trichlorophosphate 1.) room temp., 6 h, 2.) 1,2-dichloroethane, room temp., 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Croce, Piero Dalla; Rosa, Concetta La; Ritieni, Alberto
Synthesis, 1989 , # 10 p. 783 - 784
反应条件
sodium hydride in diethyl ether Ambient temperature;
参考文献
van der Stelt,C. et al.
Recueil des Travaux Chimiques des Pays-Bas, 1973 , vol. 92, p. 493 - 512
反应条件
(i) NaH, DMF, (ii) /BRN= 969568/; Multistep reaction;
参考文献
Islip; Closier; Neville
Journal of Medicinal Chemistry, 1974 , vol. 17, # 2 p. 207 - 209
