N,N-二乙基-2-丙烯酰胺合成路线 （共 23 条）
反应条件
bis[(R,R,S)-DiazaPhos-SPE]; [rhodium(I)(carbonyl)2(acetylacetonate)]; hydrogen in toluene
T=50°C; P=3375.34 Torr; 5 h; Inert atmosphereAutoclave;
参考文献
Noonan, Gary M.; Newton, David; Cobley, Christopher J.; Suarez, Andres; Pizzano, Antonio; Clarke, Matthew L.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 6 p. 1047 - 1054
反应条件
1: 100 percent / AcOH / H2O / 8 h / Heating
2: 96 percent / P4S10, NaHCO3 / 1,2-dimethoxy-ethane / 15 h / 20 °C
3: 1.) (CH3)2SO4 / 1.) 12 h, 50 deg C, acetonitrile; 2.) 15 h, 20 deg C
View Scheme
参考文献
Lombaert, Stephane De; Ghosez, Leon
Tetrahedron Letters, 1984 , vol. 25, # 32 p. 3475 - 3478
反应条件
1,4-dioxane; water; zinc; CoI2(dppe) in acetonitrile
T=80°C; 24 h;
参考文献
Wang, Chun-Chih; Lin, Pao-Shun; Cheng, Chien-Hong
Tetrahedron Letters, 2004 , vol. 45, # 32 p. 6203 - 6206
