甲基3-羟基-5-硝基-2,3-二氢-1-苯并噻吩-3-羧酸酯合成路线 (共 3 条)
反应条件
triethylamine in methanol
T=40 - 50°C; 4 h;
参考文献
UNIVERSITY OF PITTSBURGH - OF THE COMMONWEALTH SYSTEM OF HIGHER EDUCATION; WIPF, Peter; WANG, Qiming, Jan
Patent: WO2012/78859 A2, 2012 ;
Location in patent: Page/Page column 55 ;
反应条件
sodium; acetic acid in methanol; water
参考文献
Societe d'Etudes Scientifiques et Industrielles de l'Ile-de-France
Patent: US3954748 A1, 1976 ;
反应条件
potassium carbonate in water; acetone
参考文献
Societe d'Etudes Scientifiques et Industrielles de l'Ile-de-France
Patent: US3954748 A1, 1976 ;