1-(3-溴-2-甲氧基苯基)乙酮合成路线 (共 2 条)
反应条件
oxalyl dichloride in dichloromethane; dimethyl sulfoxide Swern oxidation; 0.5 h;
参考文献
Vedejs; Wang
Organic letters, 2000 , vol. 2, # 8 p. 1031 - 1032
反应条件
1.1: i-PrMgCl / tetrahydrofuran / 8 h / Heating 1.2: 84 percent / tetrahydrofuran / 0.33 h / 20 °C 2.1: 94 percent / oxaloyl chloride / CH2Cl2; dimethylsulfoxide / 0.5 h View Scheme
参考文献
Vedejs; Wang
Organic letters, 2000 , vol. 2, # 8 p. 1031 - 1032