N,N-二甲基-4-(三氟甲硫基)苯胺合成路线 （共 4 条）
反应条件
copper in N,N,N',N',N'',N''-hexamethylphosphoric triamide 160 to 175°C, 12 h;
参考文献
Remy, D. C.; Rittle, K. E.; Hunt, C. A.; Freedman, M. B.
Journal of Organic Chemistry, 1976 , vol. 41, p. 1644 - 1646
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Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.10, page 251 - 267
Full Text Show Details
Merck and Co., Inc.
Patent: US4020169 , 1977 ;
C.A., 1977 , vol. 87, p. 52939
反应条件
1: 4-(N,N-dimethylaminophenyl)diazonium tetrafluoroborate With copper(I) isothiocyanate; sodium isothiocyanate; caesium carbonate in acetonitrile T=20°C; 0.166667 h; Inert atmosphere; 2: (trifluoromethyl)-trimethylsilane in acetonitrile T=20°C; 16 h; Inert atmosphere;
参考文献
Danoun, Gregory; Bayarmagnai, Bilguun; Gruenberg, Matthias F.; Goossen, Lukas J.
Chemical Science, 2014 , vol. 5, # 4 p. 1312 - 1316
参考文献
Andreades,S. et al.
Journal of Organic Chemistry, 1964 , vol. 29, p. 898 - 900
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.5.2, page 157 - 193
