4-氯-N-甲基甲酰苯胺合成路线 （共 21 条）
参考文献
Dallacker,F.; Eschelbach,F.-E.
Justus Liebigs Annalen der Chemie, 1965 , vol. 689, p. 171 - 178
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Roberts; Vogt
Journal of the American Chemical Society, 1956 , vol. 78, p. 4778,4780
反应条件
oxygen; acetic anhydride in acetonitrile T=60°C; 20 h;
参考文献
Murata, Satoru; Tamatani, Akira; Suzuki, Kaoru; Miura, Masahiro; Nomura, Masakatsu
Chemistry Letters, 1990 , # 5 p. 757 - 760
反应条件
oxygen; acetic anhydride in acetonitrile T=30°C; 10 h;
参考文献
Murata, Satoru; Tamatani, Akira; Suzuki, Kaoru; Miura, Masahiro; Nomura, Masakatsu
Chemistry Letters, 1990 , # 5 p. 757 - 760
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate in benzene T=5 - 10°C; 1 h; Heating;
参考文献
Sharma, V. K.; Kumar, A.; Agarwal, K. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 11 p. 1153
反应条件
1: benzene / Heating 2: anhydrous potassium carbonate, sodium hydroxide, tetrabutylammmonium hydrogensulphate / benzene / 1 h / 5 - 10 °C / Heating View Scheme
参考文献
Sharma, V. K.; Kumar, A.; Agarwal, K. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 11 p. 1153
反应条件
oxygen in acetonitrile T=30°C; P=760 Torr; 10 h; other temperature, other 4-substituted N,N-dialkylanilines; Product distribution;
参考文献
Murata, Satoru; Tamatani, Akira; Suzuki, Kaoru; Miura, Masahiro; Nomura, Masakatsu
Chemistry Letters, 1990 , # 5 p. 757 - 760
反应条件
(i) KOH, EtOH, (ii) /BRN= 1209246/, toluene; Multistep reaction;
参考文献
Dallacker,F.; Eschelbach,F.-E.
Justus Liebigs Annalen der Chemie, 1965 , vol. 689, p. 171 - 178
反应条件
aluminum oxide; potassium fluoride 0.333333 h; microwave irradiation;
参考文献
Ge, Yiyu; Hu, Longqin
Tetrahedron Letters, 2007 , vol. 48, # 26 p. 4585 - 4588
反应条件
T=50°C; Substitution; 6 h; Title compound not separated from byproducts;
参考文献
Chemical Communications, , # 15 p. 1363 - 1364
反应条件
1: (COCl)2 / Ambient temperature 2: i-Pr2NEt / tetrahydrofuran / 1 h / 35 °C 3: Br2 / 2 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 10 p. 1619 - 1625
