苯并[f][1]苯并二硫杂环戊烷合成路线 （共 18 条）
反应条件
[ReBr(CO)3(thf)]2 in 1,2-dichloro-ethane
T=25°C; 9 h; Inert atmosphere;
参考文献
Kuninobu, Yoichiro; Tatsuzaki, Tomohiro; Matsuki, Takashi; Takai, Kazuhiko
Journal of Organic Chemistry, 2011 , vol. 76, # 17 p. 7005 - 7009
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene
2 h; Heating;
参考文献
Lee-Ruff, E.; Ablenas, Fred J.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1663 - 1667
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene
2 h; Heating;
参考文献
Lee-Ruff, E.; Ablenas, Fred J.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1663 - 1667
反应条件
T=650°C; P=0.01 Torr;
参考文献
Chauhan, P. M. S.; Jenkins, G.; Walker, S. M.; Storr, R. C.
Tetrahedron Letters, 1988 , vol. 29, # 1 p. 117 - 120
反应条件
1: 96 percent / 10percent sulfuric acid / ethanol / 1 h / Heating
2: 86 percent / DDQ / toluene / 2 h / Heating
View Scheme
参考文献
Lee-Ruff, E.; Ablenas, Fred J.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1663 - 1667
反应条件
T=750°C; P=0.01 Torr;
参考文献
Chauhan, P. M. S.; Jenkins, G.; Walker, S. M.; Storr, R. C.
Tetrahedron Letters, 1988 , vol. 29, # 1 p. 117 - 120
反应条件
1: 92 percent / LAH / diethyl ether
2: 23.4 mg / p-toluenesulfonic acid / toluene / 1 h / Heating
3: 86 percent / DDQ / toluene / 2 h / Heating
View Scheme
参考文献
Lee-Ruff, E.; Ablenas, Fred J.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1663 - 1667
反应条件
1: 23.4 mg / p-toluenesulfonic acid / toluene / 1 h / Heating
2: 86 percent / DDQ / toluene / 2 h / Heating
View Scheme
参考文献
Lee-Ruff, E.; Ablenas, Fred J.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1663 - 1667
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone
Yield given;
参考文献
Chauhan, P. M. S.; Jenkins, G.; Walker, S. M.; Storr, R. C.
Tetrahedron Letters, 1988 , vol. 29, # 1 p. 117 - 120
反应条件
ammonium hydroxide; zinc
参考文献
Carruthers; Crowder
Journal of the Chemical Society, 1957 , p. 1932
Full Text Show Details
Wilputte; Martin
Bulletin des Societes Chimiques Belges, 1956 , vol. 65, p. 874,891
