苯并[f][1]苯并二硫杂环戊烷合成路线 (共 18 条)
参考文献
Mayer
Justus Liebigs Annalen der Chemie, 1931 , vol. 488, p. 259,275
反应条件
T=900°C; P=0.02 Torr; 2.77778E-06 h; Product distribution;
参考文献
Ibrahim, Yehia A; Al-Awadi, Nouria A; Kaul, Kamini
Tetrahedron, 2001 , vol. 57, # 34 p. 7377 - 7381
反应条件
trifluorormethanesulfonic acid in dichloromethane
T=0 - 20°C; 2 h; Inert atmosphere;
参考文献
Rafiq, Settu Muhamad; Sivasakthikumaran, Ramakrishnan; Mohanakrishnan, Arasambattu K.
Organic Letters, 2014 , vol. 16, # 10 p. 2720 - 2723
反应条件
aluminium trichloride in 1,2-dichloro-ethane
Ambient temperature;
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1143 - 1148
反应条件
1: 80 percent / AlCl3 / 1,2-dichloro-ethane / Ambient temperature
2: 84 percent / zinc dust, conc. ammonium hydroxide / aq. NH3 / Heating
View Scheme
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1143 - 1148
反应条件
1: 80 percent / AlCl3 / 1,2-dichloro-ethane / Ambient temperature
2: 84 percent / zinc dust, conc. ammonium hydroxide / aq. NH3 / Heating
3: 84 percent / LiAlH4 / diethyl ether / Ambient temperature
View Scheme
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1143 - 1148
反应条件
1: 80 percent / AlCl3 / 1,2-dichloro-ethane / Ambient temperature
2: 84 percent / zinc dust, conc. ammonium hydroxide / aq. NH3 / Heating
3: 84 percent / LiAlH4 / diethyl ether / Ambient temperature
4: 82 percent / CrO3 / pyridine / Ambient temperature
View Scheme
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1143 - 1148
反应条件
chromium(VI) oxide; water; acetic acid
参考文献
Mayer
Justus Liebigs Annalen der Chemie, 1931 , vol. 488, p. 259,275