4,5-二氯-2-(3-三氟甲基苯基)-3(2H)哒嗪酮合成路线 (共 2 条)
反应条件
1: 3-trifluoromethyl-aniline With hydrogenchloride; sodium nitrite in water T=-5 - 0°C; 0.5 h; 2: With hydrogenchloride; tin(ll) chloride in water T=0°C; 2 h; 3: 3,4-dichloro-5-hydroxyfuran-2(5H)-one in water T=80 - 90°C;
参考文献
Zhang, Ji; Morton, Howard E.; Ji, Jianguo
Tetrahedron Letters, 2006 , vol. 47, # 49 p. 8733 - 8735
反应条件
in toluene 7 h; Heating;
参考文献
Konecny, Vaclav; Kovac, Stefan; Varkonda, Stefan
Collection of Czechoslovak Chemical Communications, 1985 , vol. 50, # 2 p. 492 - 502