1,8-二碘-3,3,4,4,5,5,6,6-辛氟辛烷合成路线 （共 8 条）
反应条件
dodecacarbonyltriiron T=100°C; P=7600 Torr; 4 h;
参考文献
Urata, Hisao; Kinoshita, Yoshihiro; Asanuma, Tatsuya; Kosukegawa, Osamu; Fuchikami, Takamasa
Journal of Organic Chemistry, 1991 , vol. 56, # 16 p. 4996 - 4999
反应条件
T=60°C; P=3102.97 Torr; 24 h;
参考文献
3M INNOVATIVE PROPERTIES COMPANY; QIU, Zai-Ming,; DAHLKE, Gregg D.,; FUKUSHI, Tatsuo,; GROOTAERT, Werner M.A.,; GUERRA, Miguel A.,
Patent: WO2012/82551 A2, 2012 ;
Location in patent: Page/Page column 13 ;
反应条件
ethanolamine; Fe3 or Fe or Co or Ru T=100°C; P=7600 Torr; Product distribution;
参考文献
Urata, Hisao; Kinoshita, Yoshihiro; Asanuma, Tatsuya; Kosukegawa, Osamu; Fuchikami, Takamasa
Journal of Organic Chemistry, 1991 , vol. 56, # 16 p. 4996 - 4999
反应条件
1: H2O / dimethylformamide 2: 53 percent / KMnO4/KOH aq. / 1.5 h / 80 °C View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 41, p. 173 - 184
反应条件
potassium hydroxide in ethylene glycol T=140°C;
参考文献
Baum, Kurt; Bedford, Clifford D.; Hunadi, Ronald J.
Journal of Organic Chemistry, 1982 , vol. 47, # 12 p. 2251 - 2257
反应条件
sodium azide in N,N-dimethyl-formamide
参考文献
Malik, A. A.; Tzeng, D.; Cheng, P.; Baum, K.
Journal of Organic Chemistry, 1991 , vol. 56, p. 3043 - 3044
反应条件
water in N,N-dimethyl-formamide
Yield given;
参考文献
Takakura, T.; Yamabe, M.; Kato, M.
Journal of Fluorine Chemistry, 1988 , vol. 41, p. 173 - 184
反应条件
1: sodium azide / dimethylformamide
2: 59 percent / hydrazine/Pd(OH)2-C / methanol / 16 h / Heating
View Scheme
参考文献
Malik, A. A.; Tzeng, D.; Cheng, P.; Baum, K.
Journal of Organic Chemistry, 1991 , vol. 56, p. 3043 - 3044
