3-[3-(二甲基氨基)丙氧基]苯甲醛合成路线 （共 3 条）
反应条件
1: With di-isopropyl azodicarboxylate; triphenylphosphine in dichloromethane T=0 - 20°C; 16 h; 2: With hydrogenchloride in water 3: With potassium carbonate in water
参考文献
Breitenbucher, J. Guy; Lee-Dutra, Alice; Neff, Danielle K.
Patent: US2006/4039 A1, 2006 ;
Location in patent: Page/Page column 14 ;
参考文献
Ahn, Gang; Schifano-Faux, Nadege; Goossens, Jean-Francois; Baldeyrou, Brigitte; Couture, Axel; Grandclaudon, Pierre; Lansiaux, Amelie; Ryckebusch, Adina
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 8 p. 2259 - 2263
反应条件
caesium carbonate in N,N-dimethyl-formamide T=50°C; 18 h;
参考文献
Patt, William C.; Cheng, Xue-Min; Repine, Joseph T.; Lee, Chet; Reisdorph, Bill R.; Massa, Mark A.; Doherty, Annette M.; Welch, Kathleen M.; Bryant, John W.; Flynn, Michael A.; Walker, Donnelle M.; Schroeder, Richard L.; Haleen, Stephen J.; Keiser, Joan A.
Journal of Medicinal Chemistry, 1999 , vol. 42, # 12 p. 2162 - 2168
