5-硝基-2-(1-吡咯烷)吡啶合成路线 （共 6 条）
反应条件
in toluene T=110°C; 2 h;
参考文献
F2G LTD
Patent: WO2009/130481 A1, 2009 ;
Location in patent: Page/Page column 140 ;
反应条件
in dimethyl sulfoxide T=25°C;
参考文献
Isanbor, Chukwuemeka; Emokpae, Thomas A.
International Journal of Chemical Kinetics, 2008 , vol. 40, # 3 p. 125 - 135
反应条件
1.1: trichlorophosphate / Reflux; Inert atmosphere 2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere 2.2: 0 - 20 °C / Inert atmosphere View Scheme
参考文献
Gruenenthal GmbH; FRANK, Robert; BAHRENBERG, Gregor; CHRISTOPH, Thomas; LESCH, Bernhard; LEE, Jeewoo
Patent: US2013/29962 A1, 2013 ;
反应条件
AgPy2MNo4 T=8 - 10°C; 0.5 h;
参考文献
Gulevskaya, Anna V.; Maes, Bert U. W.; Meyers, Caroline; Herrebout, Wouter A.; Van Der Veken, Benjamin J.
European Journal of Organic Chemistry, 2006 , # 23 p. 5305 - 5314
反应条件
potassium permanganate T=8 - 10°C;
参考文献
Verbeeck, Stefan; Herrebout, Wouter A.; Gulevskaya, Anna V.; Van Der Veken, Benjamin J.; Maes, Bert U. W.
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5126 - 5133
反应条件
in dimethyl sulfoxide T=25°C; Kinetics;
参考文献
Crampton, Michael R.; Emokpae, Thomas A.; Isanbor, Chukwuemeka
European Journal of Organic Chemistry, 2007 , # 8 p. 1378 - 1383
