1: [2-((Z)-1-Benzenesulfonyl-2-phenyl-vinyl)-phenyl]-methyl-amine With lithium hexamethyldisilazane in tetrahydrofuran T=0 - 20°C; 2: benzoyl chloride in tetrahydrofuran T=20°C; 1 h;

1: in tetrahydrofuran T=0 - 20°C; 0.166667 h; Inert atmosphere; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in tetrahydrofuran T=0°C; 0.0833333 h; Inert atmosphere;

tert.-butylhydroperoxide; copper(l) iodide; lithium chloride; palladium (II) bromide in decane; toluene T=100°C;

1.1: 88 percent / LiAlH4 / tetrahydrofuran / 3 h / 20 °C 2.1: 76 percent / tetrahydrofuran / Heating 3.1: 84 percent / Ph3P; N-bromosuccinimide / tetrahydrofuran / 2 h / 20 °C 4.1: 88 percent / dimethylformamide / 12 h / 80 °C 5.1: LHMDS / tetrahydrofuran / 0.5 h / -78 °C 5.2: tetrahydrofuran / 1 h / -78 °C 6.1: tetrahydrofuran / 2 h / 20 °C 7.1: 1.33 g / t-BuOK / tetrahydrofuran / 1 h / 0 °C 8.1: 1.06 g / aq. HCl / ethyl acetate / 2 h / 20 °C 9.1: LHMDS / tetrahydrofuran / 0 - 20 °C 9.2: 85 percent / tetrahydrofuran / 1 h / 20 °C View Scheme

1.1: diethylaluminium chloride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere 1.2: 0 °C / Inert atmosphere 2.1: tetrahydrofuran / 0.17 h / 0 - 20 °C / Inert atmosphere 2.2: 0.08 h / 0 °C / Inert atmosphere View Scheme

1.1: diethylaluminium chloride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere 1.2: 0 °C / Inert atmosphere 2.1: tetrahydrofuran / 0.17 h / 0 - 20 °C / Inert atmosphere 2.2: 0.08 h / 0 °C / Inert atmosphere View Scheme

1: 14 percent / CHCl3 / 22 h / Ambient temperature 2: 80 mg / NaH / benzene / 48 h / Ambient temperature View Scheme

1: 14 percent / CHCl3 / 22 h / Ambient temperature 2: 80 mg / NaH / benzene / 48 h / Ambient temperature View Scheme

sodium hydride in benzene 48 h; Ambient temperature;

thionyl chloride Behandeln des erhaltenen Saeurechlorids mit Benzol und Aluminiumchlorid;