反应条件
1: trichlorophosphate / 3.5 h / 110 °C / Large scale reaction
2: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 22 h / Reflux; Large scale reaction
3: water; potassium hydroxide / 1 h / 75 °C / Large scale reaction
View Scheme
参考文献
Guercio, Giuseppe; Castoldi, Damiano; Giubellina, Nicola; Lamonica, Alessandro; Ribecai, Arianna; Stabile, Paolo; Westerduin, Pieter; Dams, Riet; Nicoletti, Anna; Rossi, Sara; Bismara, Claudio; Provera, Stefano; Turco, Lucilla
Organic Process Research and Development, 2010 , vol. 14, # 5 p. 1153 - 1161