2,4-二氯-6-硝基苯胺合成路线 （共 35 条）
反应条件
sulfuric acid; acetic acid
参考文献
Berti,G. et al.
Gazzetta Chimica Italiana, 1977 , vol. 107, p. 175 - 180
反应条件
1.1: conc. sulfuric acid; aq. sodium nitrite / acetic acid / 0 °C
1.2: aq. sodium azide / 0.5 h / 20 °C
2.1: 300 mg / bis-(2-hydroxy-ethyl) ether / 1 h / 150 °C
3.1: 68 percent / triphenylphosphine / chlorobenzene / 1 h / Heating
View Scheme
参考文献
Okiyama, Natsuko; Uchiyama, Seiichi; Onoda, Maki; Imai, Kazuhiro; Santa, Tomofumi
Heterocycles, 2002 , vol. 58, p. 165 - 173
反应条件
tin(ll) chloride in ethanol
T=80°C; 1 h;
参考文献
Louvet, P.; Lallement, G.; Pernot-Marino, I.; Luu-Duc, C.; Blanchet, G.
European Journal of Medicinal Chemistry, 1993 , vol. 28, # 1 p. 71 - 75
反应条件
sodium hydrogencarbonate in ethanol; ethyl acetate
参考文献
The State of Oregon, acting by and through The Oregon State Board of Higher Education, acting for and on behalf of The Oregon Health Sciences University; The University of Oregon; The Regents of the University of California
Patent: US5514680 A1, 1996 ;
US 5514680 A
参考文献
Witt
Chemische Berichte, 1874 , vol. 7, p. 1601
Chemische Berichte, 1875 , vol. 8, p. 1226
