2-(乙酰氨基)-2-[2-(4-辛基苯基)-2-氧代乙基]-丙二酸 1,3-二乙酯合成路线 （共 3 条）
反应条件
1: triethylsilane; titanium tetrachloride / dichloromethane / 20 °C 2: lithium chloride; sodium tetrahydroborate / tetrahydrofuran; ethanol / 72.5 h / 0 - 20 °C View Scheme
参考文献
WESTFAELISCHE WILHELMS-UNIVERSITAET MUENSTER; Haufe, Guenter; Levkau, Bodo; Schaefers, Michael; Schilson, Stefani Silke; Keul, Petra
Patent: US2014/170067 A1, 2014 ;
反应条件
1: triethylsilane; titanium tetrachloride / dichloromethane / 20 °C 2: lithium chloride; sodium tetrahydroborate / tetrahydrofuran; ethanol / 72.5 h / 0 - 20 °C 3: sodium hydroxide / methanol / 5 h / |Reflux View Scheme
参考文献
WESTFAELISCHE WILHELMS-UNIVERSITAET MUENSTER; Haufe, Guenter; Levkau, Bodo; Schaefers, Michael; Schilson, Stefani Silke; Keul, Petra
Patent: US2014/170067 A1, 2014 ;
反应条件
triethylsilane; titanium tetrachloride in dichloromethane T=20°C;
参考文献
WESTFAELISCHE WILHELMS-UNIVERSITAET MUENSTER; Haufe, Guenter; Levkau, Bodo; Schaefers, Michael; Schilson, Stefani Silke; Keul, Petra
Patent: US2014/170067 A1, 2014 ;
Location in patent: Paragraph 0490; 0491; 0492; 0493; 0494; 0495; 0496 ;
