反应条件
1: potassium acetate; acetic anhydride / 4 h / Reflux
2: diisobutylaluminium hydride / dichloromethane; cyclohexane / 3.67 h / -10 - 20 °C / Inert atmosphere
3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 3 h / Inert atmosphere; Reflux
View Scheme
参考文献
Zhang, Ping; Yang, Yewei; Zheng, Xiaoliang; Huang, Wenhai; Ma, Zhen; Shen, Zhengrong
Chemical and Pharmaceutical Bulletin, 2012 , vol. 60, # 2 p. 270 - 274