N-[(2-硝基苯基)硫代]-L-苯丙氨酸合成路线 (共 9 条)
反应条件
1: 85 percent / H2O; dioxane / 2 h / Ambient temperature 2: 1 N aq. NaOH / dioxane; tetrahydrofuran / 12 h / Ambient temperature View Scheme
参考文献
Zervas,L. et al.
Journal of the American Chemical Society, 1963 , vol. 85, p. 3660 - 3666
反应条件
sodium hydroxide in 1,4-dioxane
参考文献
Zervas,L. et al.
Journal of the American Chemical Society, 1963 , vol. 85, p. 3660 - 3666
反应条件
1: Et3N / CHCl3 2: aq. NaOH / dioxane View Scheme
参考文献
Zervas,L. et al.
Journal of the American Chemical Society, 1963 , vol. 85, p. 3660 - 3666
反应条件
sodium hydroxide in tetrahydrofuran; 1,4-dioxane 12 h; Ambient temperature; Yield given;
参考文献
Romani; Bovermann; Moroder; Wunsch
Synthesis, 1985 , vol. NO. 5, p. 512 - 513
反应条件
sodium hydroxide in 1,4-dioxane
参考文献
Kricheldorf,H.R.; Fehrle,M.
Synthesis, 1974 , p. 422 - 424
参考文献
Savrda; Veyrat
Journal of the Chemical Society. Perkin transactions 1, 1970 , vol. 16, p. 2180 - 2183
反应条件
1: 94 percent / dicyclohexylcarbodi-imide, 4-dimethylaminopyridine / 1) 0 deg C, 5 min, 2) 25 deg C, 3 h 2: HCl / diethyl ether View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 19 p. 1132 - 1133
反应条件
1: 92 percent / dicyclohexylcarbodiimide, 4-dimethylaminopyridine 2: HCl / diethyl ether View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 19 p. 1132 - 1133
反应条件
1: (i) ClCO2iBu, Et3N, CHCl3, (ii) /BRN= 741933/
2: aq. NaOH / ethanol
3: HCl / ethyl acetate; acetone; diethyl ether
View Scheme
参考文献
Zervas,L. et al.
Journal of the American Chemical Society, 1963 , vol. 85, p. 3660 - 3666