2H-苯并[f]苯并三唑合成路线 （共 10 条）
反应条件
hydrogenchloride; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; hydroxylamine; oxygen in dichloromethane; water T=20°C; 3.25 h;
参考文献
Wertz, Sebastian; Studer, Armido
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 1 p. 69 - 72
参考文献
Franzen
Journal fuer Praktische Chemie (Leipzig), 1907 , vol. <2> 76, p. 224
反应条件
1: ammonia / 240 - 250 °C 2: hydrochloric acid; sodium nitrite View Scheme
参考文献
Friedlaender; Zakrzewski
Chemische Berichte, 1894 , vol. 27, p. 764
反应条件
1: 70 percent / 0.5 h / 150 - 200 °C 2: 40 percent / H4P2O7 / 150 °C View Scheme
参考文献
Molina; Vaquero; Garcia-Navio; Alvarez-Builla; De Pascual-Teresa; Gago; Rodrigo; Ballesteros
Journal of Organic Chemistry, 1996 , vol. 61, # 16 p. 5587 - 5599
反应条件
dihydrogenpyrophosphate 1) microwave heating, 10 min, 2) microwave heating, 6 min; Yield given. Multistep reaction;
参考文献
Molina, Andres; Vaquero, Juan J.; Garcia-Navio, Jose L.; Alvarez-Builla, Julio
Tetrahedron Letters, 1993 , vol. 34, # 16 p. 2673 - 2676
反应条件
1: 78 percent / 0.5 h / 150 - 200 °C 2: 64 percent / H4P2O7 / 150 °C View Scheme
参考文献
Molina; Vaquero; Garcia-Navio; Alvarez-Builla; De Pascual-Teresa; Gago; Rodrigo; Ballesteros
Journal of Organic Chemistry, 1996 , vol. 61, # 16 p. 5587 - 5599
反应条件
dihydrogenpyrophosphate 1) microwave heating, 10 min, 2) microwave heating, 5 min; Yield given. Multistep reaction;
参考文献
Molina, Andres; Vaquero, Juan J.; Garcia-Navio, Jose L.; Alvarez-Builla, Julio
Tetrahedron Letters, 1993 , vol. 34, # 16 p. 2673 - 2676
反应条件
in tetrahydrofuran; methanol 1 h; Irradiation;
参考文献
Wender, Paul A.; Touami, Sofia M.; Alayrac, Carole; Philipp, Ulrich C.
Journal of the American Chemical Society, 1996 , vol. 118, # 27 p. 6522 - 6523
反应条件
sodium dichromate; sulfuric acid
参考文献
Fries; Walter; Schilling
Justus Liebigs Annalen der Chemie, 1935 , vol. 516, p. 248,262
参考文献
Fries; Walter; Schilling
Justus Liebigs Annalen der Chemie, 1935 , vol. 516, p. 248,262
