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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
26905-24-8
合成路线
（共 37 条）
100-39-0
溴化苄
+
117744-87-3
→
反应条件
26905-24-8
反应条件
1: p-methoxyphenyl diethyldithiocarbamate With potassium hydroxide in water T=110°C; 2: benzyl bromide in water T=20°C;
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Samadi, Arash
Tetrahedron Letters, 2014 , vol. 55, # 6 p. 1212 - 1217
696-62-8
4-碘苯甲醚
+
39077-95-7
→
反应条件
831-91-4
苄基苯基硫醚
+
26905-24-8
反应条件
tetra-(n-butyl)ammonium iodide; potassium hydrogencarbonate; palladium diacetate; triphenylphosphine in 1,4-dioxane T=100°C; sulfenylation; 16 h;
参考文献
Harayama, Hiroto; Nagahama, Takayuki; Kozera, Toyohiro; Kimura, Masanari; Fugami, Keigo; Tanaka, Shuji; Tamaru, Yoshinao
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 445 - 456
104-92-7
4-溴苯甲醚
+
100-39-0
溴化苄
→
反应条件
26905-24-8
反应条件
1: 1-bromo-4-methoxy-benzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.25 h; 2: With sulfur in tetrahydrofuran; hexane T=-78°C; 3: benzyl bromide in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
Ham, Jungyeob; Yang, Inho; Kang, Heonjoong
Journal of Organic Chemistry, 2004 , vol. 69, # 9 p. 3236 - 3239
696-63-9
4-甲氧基苯硫酚
+
1207372-96-0
→
反应条件
29910-92-7
+
26905-24-8
反应条件
PPh3 gold(I) chloro complex; silver trifluoromethanesulfonate in 1,2-dichloro-ethane T=80°C; 15 h; Inert atmosphereDarkness;
参考文献
Jean, Mickael; Renault, Jacques; van de Weghe, Pierre; Asao, Naoki
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 378 - 381
696-63-9
4-甲氧基苯硫酚
→
反应条件
13141-35-0
+
26905-24-8
反应条件
PPh3 gold(I) chloro complex; silver trifluoromethanesulfonate in 1,2-dichloro-ethane T=80°C; 15 h; Inert atmosphereDarkness;
参考文献
Jean, Mickael; Renault, Jacques; van de Weghe, Pierre; Asao, Naoki
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 378 - 381
22444-88-8
→
反应条件
5335-87-5
4,4'-二甲氧基二苯二硫
+
26905-24-8
反应条件
in acetonitrile T=80°C; 22 h; Yields of byproduct given;
参考文献
Tada, Masaru; Kambe, Tohru; Inouye, Yoshinobu
Chemical Communications, 1998 , # 1 p. 41 - 42
623-12-1
4-氯苯甲醚
+
100-39-0
溴化苄
→
反应条件
26905-24-8
反应条件
palladium diacetate; potassium carbonate; thiourea; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water T=50°C; 16 h; Inert atmosphere;
参考文献
Wang, Liang; Zhou, Wei-You; Chen, Sheng-Chun; He, Ming-Yang; Chen, Qun
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 5 p. 839 - 845
623-12-1
4-氯苯甲醚
+
100-53-8
苄硫醇
→
反应条件
26905-24-8
反应条件
(SIPr)Pd(Py)Cl2; potassium tert-butylate in toluene T=100°C; 32 h; Inert atmosphere;
参考文献
Shi, Yanhui; Cai, Zhengyuan; Guan, Pei; Pang, Guangsheng
Synlett, 2011 , # 14 art. no. W09311ST, p. 2090 - 2096
696-63-9
4-甲氧基苯硫酚
+
100-51-6
苯甲醇
→
反应条件
26905-24-8
反应条件
phosphonitrilic chloride trimer T=50°C; 0.05 h; Neat (no solvent);
参考文献
Bahrami, Kiumars; Khodaei, Mohammad Mehdi; Khodadoustan, Nayere
Synlett, 2011 , # 15 art. no. B11811ST, p. 2206 - 2210
5720-07-0
4-甲氧基苯硼酸
+
100-39-0
溴化苄
→
反应条件
26905-24-8
反应条件
1: (4-methoxyphenyl)-boronic acid With potassium ethylxanthate; copper(l) chloride in methanol 3 h; Inert atmosphereReflux; 2: benzyl bromide With potassium hydroxide in methanol 3 h; Inert atmosphereReflux;
参考文献
Wang, Liang; Zhou, Wei-You; Chen, Sheng-Chun; He, Ming-Yang; Chen, Qun
Synlett, 2011 , # 20 art. no. W18411ST, p. 3041 - 3045
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