反应条件
1: With n-butyllithium; N,N,N'-trimethyl-ethylenediamine in tetrahydrofuran; hexane
T=-20°C; 24 h; Schlenk techniqueInert atmosphere;
2: With carbon tetrabromide in tetrahydrofuran; hexane
T=-43 - 20°C; 0.583333 h; Schlenk techniqueInert atmosphere;
参考文献
Grudzien, Krzysztof; Zukowska, Karolina; Malinska, Maura; Wozniak, Krzysztof; Barbasiewicz, Michal
Chemistry - A European Journal, 2014 , vol. 20, # 10 p. 2819 - 2828