3-甲基-4-(4,4,5,5-四甲基-1,3,2-二噁硼烷-2-基)苯甲酸合成路线 （共 4 条）
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; potassium acetate in N,N-dimethyl-formamide T=120°C; 0.25 h; Microwave irradiation;
参考文献
LABORATORIOS ALMIRALL, S.A.
Patent: WO2007/96072 A2, 2007 ;
Location in patent: Page/Page column 36 ;
WO 2007/096072 A2
反应条件
potassium acetate; palladium diacetate in N,N-dimethyl-formamide T=150°C; 0.5 h; Microwave irradiation;
参考文献
GLAXO GROUP LIMITED
Patent: WO2007/147109 A2, 2007 ;
Location in patent: Page/Page column 180-181 ;
WO 2007/147109 A2
反应条件
triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; 73 h;
参考文献
Commonwealth Scientific and Industrial Research Organisation
Patent: US6680401 B1, 2004 ;
Location in patent: Page column 21-22 ;
反应条件
thionyl chloride T=20°C; 4 h;
参考文献
MERCK SERONO S.A.
Patent: WO2009/43890 A1, 2009 ;
Location in patent: Page/Page column 74 ;
WO 2009/043890 A1
