2-甲氧基-5-甲氧羰基苯硼酸频那醇酯合成路线 （共 4 条）
反应条件
1: With triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; 18 h; 2: 3-iodo-4-methoxybenzoic acid methyl ester; 4,4,5,5-tetramethyl-[1,3,2]dioxaborolane in 1,4-dioxane T=80°C; 18 h;
参考文献
US6680401 B1, ;
Page column 60 ;
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; potassium acetate 18 h; RefluxInert atmosphere;
参考文献
Tetrahedron, , vol. 68, # 43 p. 8884 - 8889
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in 1,4-dioxane T=20 - 90°C; 16 h;
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 18 p. 6234 - 6253
反应条件
1: sulfuric acid / |Reflux 2: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct / 18 h / |Reflux; |Inert atmosphere View Scheme
参考文献
Tetrahedron, , vol. 68, # 43 p. 8884 - 8889
