2,6-二甲基-4-(4,4,5,5-四甲基-1,3,2-二氧硼烷-2-YL)苯酚合成路线 （共 2 条）
反应条件
1: With triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; 18 h; 2: 4-bromo-2,6-dimethyl-phenol; 4,4,5,5-tetramethyl-[1,3,2]dioxaborolane With triethylamine in 1,4-dioxane T=100°C; 336 h;
参考文献
US6680401 B1, ;
Page column 68 ;
反应条件
hydrogenchloride; water in dichloromethane
1.5 h;
参考文献
Bayer Schering Pharma AG
Patent: EP2343295 A1, 2011 ;
Location in patent: Page/Page column 23-24 ;
EP 2343295 A1
