4-乙氧基羰基甲氧基苯硼酸合成路线 (共 2 条)
反应条件
caesium carbonate in DMF (N,N-dimethyl-formamide) T=20°C; 24 h;
参考文献
WO2004/76412 A2, ;
Page 100 ;
WO 2004/076412 A2
反应条件
1: With triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; 18 h; 2: ethyl (4-bromophenoxy)acetate; 4,4,5,5-tetramethyl-[1,3,2]dioxaborolane in 1,4-dioxane T=80°C; 52 h;
参考文献
US6680401 B1, ;
Page column 69-70 ;