反应条件
1.1: 73 percent / sodium bicarbonate; sodium sulfide nonahydrate; methanol / 0.5 h / Heating 2.1: conc. aq. HCl; NaNO2 / 0.25 h / 0 °C 2.2: 84 percent / KI / H2O / Heating 3.1: 91 percent / Fe3(CO)12; methanol / toluene / 3.5 h / Heating 4.1: 83 percent / tetrakis(triphenylphosphine) palladium(0) / dimethylformamide / 2 h / 80 °C 5.1: conc. aq. HCl; NaNO2 / 0.25 h / 0 °C 5.2: 64 percent / KI / H2O / Heating 6.1: 78 percent / 3percent aq. H2O2 / 4 h / 50 °C 7.1: 82 percent / BBr3 / CH2Cl2 / 4 h / Heating View Scheme
参考文献
Reich, Siegfried H.; Johnson, Theodore; Wallace, Michael B.; Kephart, Susan E.; Fuhrman, Shella A.; Worland, Stephen T.; Matthews, David A.; Hendrickson, Thomas F.; Chan, Fora; Meador III, James; Ferre, Rose Ann; Brown, Edward L.; DeLisle, Dorothy M.; Patick, Amy K.; Binford, Susan L.; Ford, Clifford E.
Journal of Medicinal Chemistry, 2000 , vol. 43, # 9 p. 1670 - 1683
