iron(III) chloride in dichloromethane
0.5 h; Heating;
参考文献
Bedford, Robin B.; Betham, Michael; Bruce, Duncan W.; Davis, Sean A.; Frost, Robert M.; Hird, Michael
Chemical Communications, 2006 , # 13 p. 1398 - 1400
1: 67 percent / K2CO3 / dimethylformamide / 5 h / 70 °C
2: 71 percent / sodium methoxide / methanol / 1 h / 25 °C
View Scheme
参考文献
Marsilje, Thomas H.; Hedrick, Michael P.; Desharnais, Joel; Tavassoli, Ali; Zhang, Yan; Wilson, Ian A.; Benkovic, Stephen J.; Boger, Dale L.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 20 p. 4487 - 4501
magnesium
T=600°C; P=0.01 - 0.1 Torr; Title compound not separated from byproducts;
参考文献
Aitken, R. Alan; Hodgson, Philip K.G.; Morrison, John J.; Oyewale, Adebayo O.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 3 p. 402 - 415